The content presented here represents the most current version of this section, which was printed in the 24th edition of Standard Methods for the Examination of Water and Wastewater.

6630 ORGANOCHLORINE PESTICIDES

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6630 A. Introduction References
1. Zaugg SD, Sandstrom MW, Smith SG, Fehlberg KM. Methods of analysis by the U.S. Geological Survey National Water Quality Laboratory—determination of pesticides in water by C-18 solid phase extraction and capillary column gas chromatography/mass spectrometry with selected-ion monitoring. USGS Open File Report 95-181. Denver (CO): U.S. Geological Survey, Earth Science Information Center, 1995. Google Scholar
2. Stan HJ, Heberer T. Identification and confirming analysis based on gas chromatography-mass spectrometry. In: Stan HJ, ed. Analysis of pesticides in ground and surface water 1. Chemistry of plant protection. Berlin: Springer, 1995; Vol. 11, p. 141. Google Scholar
6630 B. Liquid–Liquid Extraction Gas Chromatographic Method Bibliography
Mill PA. Variation of Florisil activity: simple method for measuring absorbent capacity and its use in standardizing Florisil columns. J Assoc Offic Anal Chem. 1968;51(1):29–32. Google Scholar
Food and Drug Administration. Pesticide analytical manual. 2nd ed. Washington (DC): U.S. Department of Health, Education and Welfare, 1968; revised 1978. Google Scholar
Monsanto Chemical Company. Monsanto methodology for arochlors—analysis of environmental materials for biphenyls; Analytical Chemistry Method 71-35. St. Louis (MO): Monsanto Chemical Company; 1970. Google Scholar
U.S. Environmental Protection Agency. Method for organic pesticides in water and wastewater. Cincinnati (OH): National Environmental Research Center; 1971. Google Scholar
Steere NV, ed. Handbook of laboratory safety. Cleveland (OH): Chemical Rubber Company; 1971. Google Scholar
Goerlitz DF, Brown E. Methods for analysis of organic substances in water. In: Techniques of water resources investigations of the United States Geological Survey, Book 5, Chapter A3. Washington (DC): U.S. Department of Interior, U.S. Geological Survey; 1972, p. 24. Google Scholar
U.S. Environmental Protection Agency. Method for organochlorine pesticides in industrial effluents. Cincinnati (OH): National Environmental Research Center; 1978. Google Scholar
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6630 C. Liquid–Liquid Extraction Gas Chromatographic Method II References
1. U.S. Environmental Protection Agency. Method 608—organochlorine pesticides and PCBs. 40 CFR Part 136, 43321; Federal Regulations 49, No. 209, 1984. Google Scholar
2. U.S. Environmental Protection Agency. Determination of pesticides and PCBs in industrial and municipal wastewaters; EPA-600/4-82-023, PB82-214222. Springfield (VA): National Technical Information Service, 1982. Google Scholar
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4. Giam CS, Chan CS. Control of blanks in the analysis of phthalates in air and ocean biota samples; Special Publications 442. U.S. National Bureau of Standards, 1976. Google Scholar
5. U.S. Environmental Protection Agency. Definition and procedure for the determination of the method detection limit. 40 CFR Part 136, Appendix B. Federal Regulations 49, No. 209, 1995. Google Scholar
6. U.S. Environmental Protection Agency. Method detection limit and analytical curve studies, EPA Methods 606, 607, and 608. Special Letter Report for EPA Contract 68-03-2606. Cincinnati (OH): Environmental Monitoring and Support Laboratory, 1980. Google Scholar
7. Goerlitz CS, Law CS. Note on removal of sulfur interferences from sediment extracts for pesticide analysis. Bull Environ Contam Toxicol. 1971;6(1):9–10. Google Scholar
8. U.S. Environmental Protection Agency. Manual of analytical methods for the analysis of pesticides in human and environmental samples; EPA-600/8-80-038. Research Triangle Park (NC): Health Effects Research Laboratory, 1980. Google Scholar
9. Alford-Stevens AL, Bellar CS, Eichelberger CS, Budde CS. Characterization of commercial Aroclors by automated mass spectrometric determination of polychlorinated biphenyls by level of chlorination. Anal Chem. 1986;58(9):2014–2022. Google Scholar
10. Alford-Stevens A. Analyzing PCBs. Environ Sci Technol. 1986;20(12):1194–1199. Google Scholar
11. Alford-Stevens A. Mixture analytes. Environ Sci Technol. 1987;21(3):137–139. Google Scholar
12. Webb CS, McCall CS. Quantitative PCB standards for election capture gas chromatography. J Chromatog Sci. 1973;11(7):366–373. Google Scholar
13. U.S. Environmental Protection Agency. EPA Method Study 18, Method 608—organochlorine pesticides and PCBs; EPA-600/4-84-061, PB84-211358. Springfield (VA): National Technical Information Service, 1984. Google Scholar
Appendix—Standardization of Magnesia-Silica Gel Column by Weight Adjustment Based on Adsorption of Lauric Acid Bibliography
Mills PA. Variation of Florisil activity: simple method for measuring absorbent capacity and its use in standardizing Florisil columns. J Assoc Offic Anal Chem. 1968;51(1):29–32. Google Scholar

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Standard Methods Committee of the American Public Health Association, American Water Works Association, and Water Environment Federation. 6630 organochlorine pesticides In: Standard Methods For the Examination of Water and Wastewater. Lipps WC, Baxter TE, Braun-Howland E, editors. Washington DC: APHA Press.

DOI: 10.2105/SMWW.2882.130

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