This version is an update to the 24th edition of Standard Methods for the Examination of Water and Wastewater and was posted online April 18, 2025.

3030 PRELIMINARY TREATMENT OF SAMPLES

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3030 B. Filtration for Dissolved and Suspended Metals References
1. U.S. Environmental Protection Agency. 1994. Sample preparation procedure for spectrochemical determination of total recoverable elements; Method 200.2. Cincinnati (OH): Environmental Monitoring Systems Laboratory, 1994. Google Scholar
2. Horowitz AJ, Lum KR, Garbarino JR, Hall GEM, Lemieux C, Demas CR. Problems with using filtration to define dissolved trace element concentrations in natural water samples. Environ Sci Technol. 1996;30(3):954–963. Google Scholar
3030 D. Digestion for Metals References
1. Boumans PWJM, ed. Inductively coupled plasma emission spectroscopy, Part II: Applications and fundamentals. New York (NY): John Wiley & Sons, 1987. Google Scholar
2. U.S. Environmental Protection Agency. Test methods for evaluating solid waste, physical/chemical methods; SW-846, 3rd ed. Update 1, Methods 3005A, 3010A, 3020A & 3050A. Washington DC: Office of Solid Waste & Emergency Response; 1992. Google Scholar
3. Hoenig M, de Kersabiec AM. Sample preparation steps for analysis by atomic spectroscopy methods: present status. Spectrochim Acta B. 1996;51(11):1297–1307. Google Scholar
4. Jarvis KE, Gray AL, Houk RS, eds. Sample preparation for ICP-MS. In Handbook of inductively coupled plasma mass spectrometry. London, UK: Blackie; 1992, Ch. 7. Google Scholar
5. U.S. Environmental Protection Agency. Sample preparation procedure for spectrochemical determination of total recoverable elements; Method 200.2. Cincinnati (OH): Environmental Monitoring Systems Laboratory; 1994. Google Scholar
6. Kingston HM, Haswell S, eds. Microwave enhanced chemistry: Fundamentals, sample preparation and applications. Washington DC: American Chemical Society; 1997. Google Scholar
7. Bock R. A Handbook of decomposition methods in analytical chemistry. Glasgow (UK): Blackie; 1979. Google Scholar
3030 E. Nitric Acid Digestion Reference
1. Jarvis KE, Gray AL, Houk RS, eds. Sample preparation for ICP-MS. In: Handbook of inductively coupled plasma mass spectrometry. London (UK): Blackie and Son, Ltd.; Chapter 7, 1992. Google Scholar
3030 K. Microwave-Assisted Digestion References
1. Kingston HM, Haswell S, eds. Microwave enhanced chemistry: fundamentals, sample preparation and applications. Washington DC: American Chemical Society; 1997. Google Scholar
2. U.S. Environmental Protection Agency. Microwave assisted acid digestion of aqueous samples and extracts; SW-846. Method 3015, Test Methods for Evaluating Solid Waste. Washington DC: U.S. Environmental Protection Agency; 1990. Google Scholar

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Standard Methods Committee of the American Public Health Association, American Water Works Association, and Water Environment Federation. 3030 preliminary treatment of samples In: Standard Methods For the Examination of Water and Wastewater. Lipps WC, Baxter TE, Braun-Howland E, editors. Washington DC: APHA Press.

DOI: 10.2105/SMWW.2882.041

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