This version is an update to the 24th edition of Standard Methods for the Examination of Water and Wastewater and was posted online April 18, 2025.

6651 GLYPHOSATE HERBICIDE

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6651 A. Introduction References
1. Moye HA, Miles CJ, Scherer SJ. A simplified high-performance liquid chromatographic residue procedure for the determination of glyphosate herbicide and (aminomethyl) phosphonic acid in fruits and vegetables employing postcolumn fluorogenic labeling. J Agric Food Chem. 1983;31(1):69–72. Google Scholar
2. Cowell JE, Kunstman JL, Nord PJ, Steinmetz JR, Wilson GR. Validation of an analytical residue method for analysis of glyphosate and metabolite: an interlaboratory study. J Agric Food Chem. 1986;34(6):955–960. Google Scholar
3. Oppenhuizen ME, Cowell JE. Liquid chromatographic determination of glyphosate and aminomethylphosphonic acid in environmental water: collaborative study. J Assoc Offic Anal Chem. 1991;74(2):317–323. Google Scholar
4. Deyrup CL, Chang SM, Weintraub RA, Moye HA. Simultaneous esterification and acylation of pesticides for analysis by gas chromatography. 1. Derivatization of glyphosphate and (aminomethyl) phosphonic acid with fluorinated alcohol-perfluorinated anhydrides. J Agric Food Chem. 1985;33(5):944–947. Google Scholar
6651 A. Introduction Bibliography
Bardalaye PC, Wheeler WB, Hoye HA. Analytical techniques of glyphosate residue analysis. In: Grossbard E, Atkinson D, eds. The Herbicide Glyphosate. Woburn (MA): Butterworths; 1985. Google Scholar
6651 B. Liquid Chromatographic Post-Column Fluorescence Method References
1. Cowell JE, Kunstman JL, Nord PJ, Steinmetz JR, Wilson GR. Validation of an analytical residue method for analysis of glyphosate and metabolite: an interlaboratory study. J Agric Food Chem. 1986;34(6):955–960. Google Scholar
2. Moye HA, Miles CJ, Scherer SJ. A simplified high-performance liquid chromatographic residue procedure for the determination of glyphosate herbicide and (aminomethyl) phosphonic acid in fruits and vegetables employing postcolumn fluorogenic labeling. J Agric Food Chem. 1983;31(1):69–72. Google Scholar
3. Selvaka CM, Jiao KS, Krull IS. Construction and comparison of open tubular reactors for post-column reaction detection in liquid chromatography. Anal Chem. 1987;59(17):2221–2224. Google Scholar
4. Oppenhuizen ME, Cowell JE. Liquid chromatographic determination of glyphosate and aminomethylphosphonic acid in environmental water: collaborative study. J Assoc Offic Anal Chem. 1991;74(2):317–323. Google Scholar

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Standard Methods Committee of the American Public Health Association, American Water Works Association, and Water Environment Federation. 6651 glyphosate herbicide In: Standard Methods For the Examination of Water and Wastewater. Lipps WC, Baxter TE, Braun-Howland E, editors. Washington DC: APHA Press.

DOI: 10.2105/SMWW.2882.132

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